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    2019-10-1 · The aim of the current research is to investigate the low-temperature sintering of a nano-crystalline lithium-mica glass-ceramic. Sol-gel technique was used to prepare the glass-ceramics by application of LiMg 3 AlSi 3(1+x) O 10+6x F 2 with various x values (0.25, 0.5, 0.75, and 1) and different amounts of MgF 2 as the sintering aid. Use of appropriate amounts of additive and stoichiometric ...

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  • Korean Journal of Metals and Materials

    2018-1-24 · Moreover, it was determined that the optimum operating conditions which offer a high purity level of magnesium and reduce the degree of vapor was the case 5 (1200 ℃, 0.1 ~ 0.01 torr). In addition, the distribution of solid impurities in the Mg crown was calculated by a multi-stage calculation method while decreasing the temperature.

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